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Diffraction Group
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E-Mail: sinq@psi.ch -

DMC: COLD NEUTRON POWDER DIFFRACTOMETER



DMC




    Technical Specifications


    Sample environment

  • 3He/4He dilution refrigerator, Tmin = 50 mK
  • He cryostats, 1.5 K ≤ T ≤ 325 K
  • Cryo-furnace, 2 K ≤ T ≤ 600 K
  • Closed-cycle cooling machines, 15 K ≤ T ≤ 475 K
  • Cryo-magnet MA6, 2.8 Tesla (vertical), 1.8 K ≤ T ≤ 300 K
  • Cryo-magnet MA4, 4 Tesla (vertical), 4.2 K ≤ T ≤ 80 K
  • Cryo-magnet MA02, 1.8 Tesla (horizontal), 1.8 K ≤ T ≤ 300 K
  • Furnaces, Tmax = 1800 K
  • Clamp pressure cell, Pmax = 15 kbar, 2 K ≤ T ≤ 300 K
  • Paris-Edinburgh press (opposed anvils), Pmax = 100 kbar, 3 K ≤ T ≤ 300 K

    Position

  • Guide hall, at the cold neutron guide RNR12, supermirrorguide (m=2, height 12 cm, width 2 cm)

    Monochromators

  • Pyrolythic Graphite (002), vertically focusing, 5 crystals of 2.5 cm height
  • Germanium (311, 511, 400), vertically focusing, 9 crystals of 1.4 cm height (optional)

    Wavelengths

  • Any wavelength between 2.3 Å and 6 Å is possible, standard wavelengths (PG002 monochromator) are 2.45 Å, 3.8 Å, 4.2 Å and 4.5 Å

    Collimations

  • Optional primary and secondary collimation (Gd-O Soller collimators)
  • Oscillating collimator system between sample and detector: 73 Cd coated steel plates of 0.02 cm thickness, angular distance 1.2°

    Detector system

  • "Banana" type multidetector, linear position-sensitive BF3 counter (LCC 400CP, Thompson-CSF)
  • 400 detectors with angular separation of 0.2°, covering simultaneously a scattering angle range of 79.8°, radius 1.5 m
  • positioning of detector on air cushions for intermediate steps or larger scattering angle range

    Instrument software

  • SICS (SINQ Instrument Control Software) for control of the measurement
  • SEA, TECS (Temperature Control Software) for control of sample environment
  • FIT, FULLPROF, ... for data analysis

    Resolution and Q-Range

    DMC Resolution